van de Kamp T., Schwermann A.H., dos Santos Rolo T., Losel P.D., Engler T., Etter W., Farago T., Gottlicher J., Heuveline V., Kopmann A., Mahler B., Mors T., Odar J., Rust J., Tan Jerome N., Vogelgesang M., Baumbach T., Krogmann L.

in Nature Communications, 9 (2018), 3325. DOI:10.1038/s41467-018-05654-y

Abstract

© 2018, The Author(s). About 50% of all animal species are considered parasites. The linkage of species diversity to a parasitic lifestyle is especially evident in the insect order Hymenoptera. However, fossil evidence for host–parasitoid interactions is extremely rare, rendering hypotheses on the evolution of parasitism assumptive. Here, using high-throughput synchrotron X-ray microtomography, we examine 1510 phosphatized fly pupae from the Paleogene of France and identify 55 parasitation events by four wasp species, providing morphological and ecological data. All species developed as solitary endoparasitoids inside their hosts and exhibit different morphological adaptations for exploiting the same hosts in one habitat. Our results allow systematic and ecological placement of four distinct endoparasitoids in the Paleogene and highlight the need to investigate ecological data preserved in the fossil record.

Blank T., Pfistner P., Leyrer B., Caselle M., Simons C., Schmidt C.J., Weber M.

in 2018 International Conference on Electronics Packaging and iMAPS All Asia Conference, ICEP-IAAC 2018 (2018) 288-292. DOI:10.23919/ICEP.2018.8374306

Abstract

© 2018 Japan Institute of Electronics Packaging. The Compressed Baryonic Matter Experiment (CBM) investigates highly compressed nuclear matter, utilizing a Silicon Tracking System comprising 896 silicon sensors modules packed in eight layers with an overall area of four sqm. Each module consists of one sensor, 16 Read-Out Chips and 16 double-layer micro flex-cables, which are connected to the top and bottom side of the sensor. The cables are up to 50 cm long. They carry 128 signal traces on two layers at a pitch of 100 μm and a line-width of 25 μm. The layers are separated by a meshed core to reduce the cable capacity to 0.44 pF/cm. The cables are bonded onto one sensor by a pick and place flip-chip machine. The interconnection is realized by gold stud-bumps on the silicon and SAC solder bumps on the cable. The status of the sensor module and cable production process are presented.

Rolo T.S., Reich S., Karpov D., Gasilov S., Kunka D., Fohtung E., Baumbach T., Plech A.

in Applied Sciences (Switzerland), 8 (2018), 737. DOI:10.3390/app8050737

Abstract

© 2018 by the authors. An array of compound refractive X-ray lenses (CRL) with 20 × 20 lenslets, a focal distance of 20 cm and a visibility of 0.93 is presented. It can be used as a Shack-Hartmann sensor for hard X-rays (SHARX) for wavefront sensing and permits for true single-shot multi-contrast imaging the dynamics of materials with a spatial resolution in the micrometer range, sensitivity on nanosized structures and temporal resolution on the microsecond scale. The object’s absorption and its induced wavefront shift can be assessed simultaneously together with information from diffraction channels. In contrast to the established Hartmann sensors the SHARX has an increased flux efficiency through focusing of the beam rather than blocking parts of it. We investigated the spatiotemporal behavior of a cavitation bubble induced by laser pulses. Furthermore, we validated the SHARX by measuring refraction angles of a single diamond CRL, where we obtained an angular resolution better than 4 μrad.

Ametova E., Ferrucci M., Chilingaryan S., Dewulf W.

in Measurement Science and Technology, 29 (2018), 065007. DOI:10.1088/1361-6501/aab1a1

Abstract

© 2018 IOP Publishing Ltd. The recent emergence of advanced manufacturing techniques such as additive manufacturing and an increased demand on the integrity of components have motivated research on the application of x-ray computed tomography (CT) for dimensional quality control. While CT has shown significant empirical potential for this purpose, there is a need for metrological research to accelerate the acceptance of CT as a measuring instrument. The accuracy in CT-based measurements is vulnerable to the instrument geometrical configuration during data acquisition, namely the relative position and orientation of x-ray source, rotation stage, and detector. Consistency between the actual instrument geometry and the corresponding parameters used in the reconstruction algorithm is critical. Currently available procedures provide users with only estimates of geometrical parameters. Quantification and propagation of uncertainty in the measured geometrical parameters must be considered to provide a complete uncertainty analysis and to establish confidence intervals for CT dimensional measurements. In this paper, we propose a computationally inexpensive model to approximate the influence of errors in CT geometrical parameters on dimensional measurement results. We use surface points extracted from a computer-aided design (CAD) model to model discrepancies in the radiographic image coordinates assigned to the projected edges between an aligned system and a system with misalignments. The efficacy of the proposed method was confirmed on simulated and experimental data in the presence of various geometrical uncertainty contributors.

Reich S., Dos Santos Rolo T., Letzel A., Baumbach T., Plech A.

in Applied Physics Letters, 112 (2018), 151903. DOI:10.1063/1.5022748

Abstract

© 2018 Author(s). We demonstrate the fabrication of a 2D Compound Array Refractive Lens (CARL) for multi-contrast X-ray imaging. The CARL consists of six stacked polyimide foils with each displaying a 2D array of lenses with a 65 μm pitch aiming for a sensitivity on sub-micrometer structures with a (few-)micrometer resolution in sensing through phase and scattering contrast at multiple keV. The parabolic lenses are formed by indents in the foils by a paraboloid needle. The ability for fast single-exposure multi-contrast imaging is demonstrated by filming the kinetics of pulsed laser ablation in liquid. The three contrast channels, absorption, differential phase, and scattering, are imaged with a time resolution of 25 μs. By changing the sample-detector distance, it is possible to distinguish between nanoparticles and microbubbles.

Cavadini P., Weinhold H., Tonsmann M., Chilingaryan S., Kopmann A., Lewkowicz A., Miao C., Scharfer P., Schabel W.

in Experiments in Fluids, 59 (2018), 61. DOI:10.1007/s00348-017-2482-z

Abstract

© 2018, Springer-Verlag GmbH Germany, part of Springer Nature. To understand the effects of inhomogeneous drying on the quality of polymer coatings, an experimental setup to resolve the occurring flow field throughout the drying film has been developed. Deconvolution microscopy is used to analyze the flow field in 3D and time. Since the dimension of the spatial component in the direction of the line-of-sight is limited compared to the lateral components, a multi-focal approach is used. Here, the beam of light is equally distributed on up to five cameras using cubic beam splitters. Adding a meniscus lens between each pair of camera and beam splitter and setting different distances between each camera and its meniscus lens creates multi-focality and allows one to increase the depth of the observed volume. Resolving the spatial component in the line-of-sight direction is based on analyzing the point spread function. The analysis of the PSF is computational expensive and introduces a high complexity compared to traditional particle image velocimetry approaches. A new algorithm tailored to the parallel computing architecture of recent graphics processing units has been developed. The algorithm is able to process typical images in less than a second and has further potential to realize online analysis in the future. As a prove of principle, the flow fields occurring in thin polymer solutions drying at ambient conditions and at boundary conditions that force inhomogeneous drying are presented.

Zakharova M., Vlnieska V., Fornasier H., Borner M., dos Santos Rolo T., Mohr J., Kunka D.

in Applied Sciences (Switzerland), 8 (2018), 468. DOI:10.3390/app8030468

Abstract

© 2018 by the authors. Single-shot grating-based phase-contrast imaging techniques offer additional contrast modalities based on the refraction and scattering of X-rays in a robust and versatile configuration. The utilization of a single optical element is possible in such methods, allowing the shortening of the acquisition time and increasing flux efficiency. One of the ways to upgrade single-shot imaging techniques is to utilize customized optical components, such as two-dimensional (2D) X-ray gratings. In this contribution, we present the achievements in the development of 2D gratings with UV lithography and gold electroplating. Absorption gratings represented by periodic free-standing gold pillars with lateral structure sizes from 5 μm to 25 μm and heights from 5 μm to 28 μm have shown a high degree of periodicity and defect-free patterns. Grating performance was tested in a radiographic setup using a self-developed quality assessment algorithm based on the intensity distribution histograms. The algorithm allows the final user to estimate the suitability of a specific grating to be used in a particular setup.

Sakraker Ozmen I., Joshi A., Bohrk H., Hanschke D., Cecilia A.

in 2018 Joint Thermophysics and Heat Transfer Conference (2018), AIAA 2018-3588. DOI:10.2514/6.2018-3588

Abstract

© 2018 by Isil Sakraker Özmen, Archana Joshi, Hannah Boehrk, Daniel Haenschke, Angelica Cecilia. Published by the American Institute of Aeronautics and Astronautics, Inc. The cork based DLR Cork and low density DLR ZURAM materials were exposed to heat while being monitored by x-ray radiation in a synchrotron facility. A portable furnace was manufactured to provide the low pressure conditions of the atmospheric entry and the high stagnation heat fluxes. A total of 4 samples were exposed to radiative heating at 10.4 mbar pressure. The sample was rotated inside the furnace by a miniature servomotor to allow for 3D image reconstruction. Furthermore, 2D radiography sequences were also acquired with stationary samples. The charring, char front propagation and volumetric expansion were prominent in the case of DLR Cork. Even though the ZURAM sample did not significantly char, volumetric phenomena were observed even in the virgin regions. 3D image sequences are provided for ablating DLR Cork material, where the surface topology evolution can be observed. Furthermore, individual cork granules could be tracked throughout the ablation. An optical flow analysis was applied to track the carbon fibers following the volumetric phenomena inside the DLR ZURAM samples.

Ametova E., Ferrucci M., Chilingaryan S., Dewulf W.

in Precision Engineering (2018). DOI:10.1016/j.precisioneng.2018.05.016

Abstract

© 2018 Elsevier Inc. X-ray computed tomography (CT) is an imaging technique that allows the reconstruction of an imaged part in the form of a three-dimensional attenuation map. The CT data acquisition process consists of acquiring X-ray transmission images from multiple perspectives. Analysis of the reconstructed attenuation map can provide dimensional and material information about the measured part(s). Therefore, CT is recognized as a solution for quality control tasks, for example dimensional inspection of complex objects with intricate inner geometries. CT measurements can suffer from various sources of error in the measurement procedure. One such influence is the geometrical alignment of the CT instrument components. Typical tomographic reconstruction algorithms impose strict requirements on the relative position and orientation of the three main components: X-ray source, rotation axis of the sample stage, and X-ray detector. Any discrepancy in the actual CT geometry from the geometry assumed by the reconstruction algorithm will contribute to errors in measurements performed on the reconstructed data. There is currently no standardized or easily implementable method for users to compensate geometrical misalignments of the CT instrument. In many cases, the procedure of mechanical adjustment of CT instrument is time consuming and impractical. In this paper, we show that software-based compensation of deviations in CT instrument geometry is an effective alternative to mechanical adjustment of CT instrument. Through computer simulations, we compare qualitatively and quantitatively two methods to compensate CT instrument misalignment: radiographic re-binning (interpolation) and a modified conventional reconstruction algorithm with embedded misalignment compensation.

Jerome N.T., Kopmann A.

in VISIGRAPP 2018 – Proceedings of the 13th International Joint Conference on Computer Vision, Imaging and Computer Graphics Theory and Applications, 3 (2018) 341-348.

Abstract

© 2018 by SCITEPRESS – Science and Technology Publications, Lda. All rights reserved. With the advancement of instrument precision, research facilities are generating data at an unprecedented rate. These experimental results are stored in a digital library platform which the contents are later accessible from within the facility or the public. However, the sheer volume of collected data is overwhelming the capacity of researchers and impedes the process of browsing for the desired data. In this paper, we present a concept of Digital Visual Exploration Library (DVEL) based on the confluence of two major research domains-digital library and visualisation-that enables efficient browsing of the growing data within a digital library. We complement the current state-of-the-art textual metadata description by integrating visual exploration to address big complex data, i.e., data of large size, multimodal data and multivariate data. We describe our concept based on use cases from three unique domains: climate research with Doppler wind lidar, X-ray-imaging for entomology research, and medical imaging with ultrasound computer tomography.